Another P2P Synthesis

Author

Topic: Another P2P Synthesis

Wizard X
PimpBee

posted 02-11-2000 08:29 PM

C6H5CH2MgBr + CH3CO2Na
====[ether/25degC/24Hrs]======>
C6H5CH2-C(=O)-CH3 + NaOMgBr

P2P is only 25%

C6H5CH2Li + CH3CO2Li
====[ether/25degC/6Hrs]======>
C6H5CH2-C(=O)-CH3 + Li2O

P2P is only 62-63%

C6H5CH2CO2Li + CH3Li
====[ether/25degC/2-3Hrs]======>
C6H5CH2-C(=O)-CH3 + Li2O

P2P is only 69%

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